African Journal of Agriculture

ISSN 2375-1134

African Journal of Agriculture ISSN 2375-1134 Vol. 6 (1), pp. 001-004, January, 2019. © International Scholars Journals

Full Length Research Paper

Determination of residues of deltaméthrin in wheat and potato by HPLC

Rachdi BOUSSAHEL* 1 , Khadija M. MOUSSAOUI 2 , Djamila HARIK 2

1H. C. A., Service de Toxicologie, BP 240 Kouba 16050, Algeria.

2Ecole Nationale Polytechnique, El Harrach 16200, Algeria

Accepted 2 November, 2018

Abstract

Residues of deltamethrin, a pyrethroid insecticide commonly used to protect stored grains, have been determined in wheat and potato by high -performance liquid chromatography with UV detection at 233 nm after extraction by chloroform and a silica gel clean-up. Recoveries from fortified samples spiked with 1 ppm of deltamethrin exceeded 75% for both products. The control carried out on imported products showed the presence of this insecticide that sometimes exceeded the maximum limits of residues authorized by the OMS/FAO (0.10 ppm in potatoes and 1.00 in wheat).

Key words: deltamethrin, residues, wheat, potato, HPLC.